Notes d'application Amlopidine Besylate
Surf C18 Extreme 100 A 5µm. P/N : 15046-5-SU-C18EX
Echantillon Amlopidine Besylate (Méthode EP 1491).
Conditions:
Ø 4,6x150mm 5µm - H2O AmAc / MeOH (30:70) - 1,5ml/min - 237 nm - Pression 2000 psi. (EP 1491).
| Peak Name | RT | (µV.sec) | % Area | K Prime | USP Tailing |
| Impureté F | 2,902 | 9289 | 0,07 | 2,87 | 1,1 |
| Amlodipine Besylate |
3,684 | 12455696 | 99,9 | 3,91 | 1,91 |
| Impureté E | 4,948 | 2400 | 0,02 | 5,6 |
Notes d'application Caféine
Surf C18 AQ 100 A 3µm 150x4.6 mm P/N : 15046-3-SU-C18AQ
Echantillon Caféine depuis café instantanné.
Conditions:
Eau - 0.5 % FA - 30 mM AmFm 95 % | Acetonitrile - 5 % |1 ml /min | l = 272 nm
| RT | |
| 1 | 11,3563 |
| 2 | 11,3462 |
| 3 | 11,3214 |
| 4 | 11,3431 |
| 5 | 11,3464 |
| 6 | 11,3464 |
| % RSD | 0,1 |
Note d'application Nicotine
Surf C18 AQ 100 A 3µm 150x4.6 mm | P/N : 15046-3-SU-C18AQ
Echantillon Nicotine Liquide mentholé de e-cigarette.
Conditions:
Eau - 0.5 % FA - 30 mM AmFm 95 % | Acetonitrile - 5 % |1 ml /min | l = 260 nm
| RT | |
| 1 | 4,1905 |
| 2 | 4,1881 |
| 3 | 4,1734 |
| 4 | 4,1890 |
| % RSD | 0,2 |
